Free Ebook 150 and More Basic NMR Experiments: A Practical Course, by Siegmar Braun, Hans-Otto Kalinowski, Stefan Berger
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150 and More Basic NMR Experiments: A Practical Course, by Siegmar Braun, Hans-Otto Kalinowski, Stefan Berger
Free Ebook 150 and More Basic NMR Experiments: A Practical Course, by Siegmar Braun, Hans-Otto Kalinowski, Stefan Berger
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Explore the full productivity of your NMR equipment! - How one has to perform NMR experiments? - Which experiment conveys the desired information? - How do the applied pulse sequences work? - How can the desired informations be read off the spectra? - Which equipment is needed for special experiments? The new edition of this highly successful book is expanded by another 50 important NMR experiments dedicated to the latest developments. The expansions mainly concern the fields of chemical applications, of very recent gradient selected experiments now arranged in two chapters (1D and 2D), and of the basics of solid-state NMR in a completely new chapter. Again, all experiments from basic pulse determinations to advanced 2D and some 3D techniques have been performed especially for this book. The figures are taken directly from the spectrometer output and the reader can therefore rely on the results presented. Written by leading experts, it is a thorough guide through the maze of modern NMR tools. Being a textbook as well as a reference and work book for the laboratory, this book is a must for every scientist applying NMR as well as for students preparing for their lab courses.
- Sales Rank: #3167171 in Books
- Published on: 1998-09-10
- Ingredients: Example Ingredients
- Original language: English
- Number of items: 1
- Dimensions: 9.59" h x 1.22" w x 6.65" l, .0 pounds
- Binding: Paperback
- 610 pages
Review
From reviews of "100 and More Basic NMR Experiments":
... an essential purchase for all NMR devotees ... honest, well focused and most adequately produced ... A wealth of information is clearly expressed and provided. Post-graduate students will find it of particular value.
Analyst
...an excellent tool for any practising NMR spectroscopist...
The Analyst
From the Publisher
From the Back Cover
Explore the full productivity of you NMR equipment!
How to perform NMR experiments? Which experiment conveys the desired information? How do the applied pulse sequences work? How can the desired information be read off the spectra? Which equipment is needed for special experiments?
The new edition of this highly successful book is expanded by another 50 important NMR experiments dedicated to the latest developments. The expansion mainly concerns the fields of chemical applications of very recently developed gradient-selected experiments now arranged in two chapters (1D and 2D). Moreover, the basics of solid-state NMR are covered in a completely new chapter.
Again, all experiments from basic pulse determinations to advanced 2D and some 3D techniques have been performed especially for this book. The figures are taken directly from the spectrometer output and the reader can therefore rely on the results presented.
Written by leading experts, this book is a thorough guide through the maze of modern NMR tools. Being a textbook as wall as a reference and work book for the laboratory, it is a must for every scientist applying NMR as well as for students preparing for their lab courses.
From the Back Cover
S. Braun, H.-O. Kalinowski, S. Berger 150 and More Basic NMR Experiments A Practical Course Explore the full productivity of your NMR equipment!
- How to perform NMR experiments?
- Which experiment conveys the desired information?
- How do the applied pulse sequences work?
- How can the desired information be read off the spectra?
- Which equipment is needed for special experiments?
Most helpful customer reviews
4 of 4 people found the following review helpful.
As the title says, your basic NMR spectroscopy catelog.
By A Customer
NMR spectroscopy is a powerful tool for chemists interested in structure, dynamics and function of molecular systems. The success of this technique has lead to a proliferation of experiments yielding a wealth of data about chemical structure ranging from small molecules to not-so-small proteins and beyond. The authors have compiled a core of NMR experiments that will serve a student new to the field or an old-hand who has forgotten the phase-cycle of a particular pulse sequence. The book is sectioned into 14 chapters with the 1st two being introductory ( What is a NMR spectrometer and why is it sitting away from everything else? or If I have radiation dampening do I need to get a mop?). The next 10 chapters take the reader from routine spectroscopy experiments to a variety of 1- and 2- dimensional liquid NMR experiments with and without magnetic field gradients. The last two chapters introduce the reader to some basic 3-dimensional liquid sequences and solids NMR spectroscopy. These two subjects could have been extended but I imagine we will see that in the next volume, 150 to 300 NMR experiments. There are 160 (according to my count) different experiments and measurements discussed and each is organized to familarize the experimenter with the purpose of the experiment, the procedure to perform it, and some expected results for the experiment. The authors have wisely included a readers observation area for each section. This allows the utility of the book to grow as the reader gains experience with each NMR method. This book should be in any NMR laboratory and would be an added help to any course using NMR spectroscopy. I know any undergraduate organic chemistry course should get an attendance boost from experiment 8.15 where the students would determine the alcohol content in polish vodka. (As a student I would have suggested a more hands on approach.) The final upshot is this is an great compendium and should be a staple in any NMR laboratory period.
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